Mo(17)O2(acac)2

Base Information

Chemical Name:Mo(17)O2(acac)2
CAS No.:109309-22-0
Molecular Formula:C₁₀H₁₄MoO₆
Molecular Weight:328.159
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mo(17)O2(acac)2

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Technology Process of Mo(17)O2(acac)2

There total 2 articles about Mo(17)O2(acac)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 7631-95-0
sodium molybdate dihydrate

: 123-54-6,81235-32-7
acetylacetone

: 13968-48-4
¹⁷O-water

: 109309-22-0
Mo(17)O2(acac)2

Guidance literature:: With HCl; In water; Mo-compd. incubated anaerobically with H2O ((16):(17):(18)O = 12.95:51.48:35.57) overnight, addn. of acetylacetone, dropwise addn. of HCl, stirred for 24 h; filtered, washed with H2O, n-BuOH and Et2O, dried under vac.; enriched to 50 atom% in (17)O;
DOI:10.1021/ja00253a016

Reference yield:

: sodium molybdate

: 123-54-6,81235-32-7
acetylacetone

: 13968-48-4
¹⁷O-water

: 109309-22-0
Mo(17)O2(acac)2

Guidance literature:: With hydrogenchloride; In further solvent(s); a soln. of Na2MoO4 in H2(17)O stirred for 15 h, ligand added, a soln. ofHCl added dropwise until the soln. pH 2, stirred for 24 h; filtered off, washed (H2O, pentane, Et2O);
DOI:10.1021/ja801406f