4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde

Base Information

Chemical Name:4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde
CAS No.:78647-57-1
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:237.26
Hs Code.:

Synonyms:

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Chemical Property of 4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde

Chemical Property:

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Technology Process of 4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde

There total 10 articles about 4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7149-92-0
2,4-dimethoxy-3-methylbenzaldehyde

: 78647-57-1
4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium deuteride / diethyl ether / 3 h / Ambient temperature

2: hydrogen / palladium oxide / acetic acid

3: stannic chloride / CS₂ / 2 h / Heating

4: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature

5: toluene-p-sulphonic acid / 130 - 140 °C / 0.4 Torr

6: ozone, dimethyl sulphide / ethyl acetate / 0.17 h / -78 °C

7: boron tribromide / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; lithium aluminium deuteride; dimethylsulfide; hydrogen; boron tribromide; tin(IV) chloride; toluene-4-sulfonic acid; ozone; palladium(II) oxide; In carbon disulfide; diethyl ether; dichloromethane; acetic acid; ethyl acetate;
DOI:10.1039/P19810001685

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 78647-57-1
4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) hydrogen chloride gas, 2.) water / 1.) ether, 45 min, 2.) 40 deg C

2: 92 percent / potassium carbonate / acetone / 5 h / Heating

3: lithium aluminium deuteride / diethyl ether / 3 h / Ambient temperature

4: hydrogen / palladium oxide / acetic acid

5: stannic chloride / CS₂ / 2 h / Heating

6: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature

7: toluene-p-sulphonic acid / 130 - 140 °C / 0.4 Torr

8: ozone, dimethyl sulphide / ethyl acetate / 0.17 h / -78 °C

9: boron tribromide / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; lithium aluminium deuteride; dimethylsulfide; water; hydrogen; boron tribromide; tin(IV) chloride; potassium carbonate; toluene-4-sulfonic acid; ozone; palladium(II) oxide; In carbon disulfide; diethyl ether; dichloromethane; acetic acid; ethyl acetate; acetone;
DOI:10.1039/P19810001685

Reference yield:

: 6248-20-0
2,4-dihydroxy-3-methylbenzaldehyde

: 78647-57-1
4,6-dihydroxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde

Guidance literature:: Multi-step reaction with 8 steps

1: 92 percent / potassium carbonate / acetone / 5 h / Heating

2: lithium aluminium deuteride / diethyl ether / 3 h / Ambient temperature

3: hydrogen / palladium oxide / acetic acid

4: stannic chloride / CS₂ / 2 h / Heating

5: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature

6: toluene-p-sulphonic acid / 130 - 140 °C / 0.4 Torr

7: ozone, dimethyl sulphide / ethyl acetate / 0.17 h / -78 °C

8: boron tribromide / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; lithium aluminium deuteride; dimethylsulfide; hydrogen; boron tribromide; tin(IV) chloride; potassium carbonate; toluene-4-sulfonic acid; ozone; palladium(II) oxide; In carbon disulfide; diethyl ether; dichloromethane; acetic acid; ethyl acetate; acetone;
DOI:10.1039/P19810001685