Technology Process of C37H46N5O14P
There total 11 articles about C37H46N5O14P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 92 percent / NH2OH*HCl, Et3N, molecular sieves / tetrahydrofuran
2: 100 percent / NaBH3CN / acetic acid
3: 87 percent / Et3N / tetrahydrofuran
4: 92 percent / LiOH / methanol
5: 1) POCl3, pyridine / 1) THF, 2) THF
With
pyridine; lithium hydroxide; molecular sieve; hydroxylamine hydrochloride; sodium cyanoborohydride; triethylamine; trichlorophosphate;
In
tetrahydrofuran; methanol; acetic acid;
DOI:10.1016/0960-894X(96)00169-2
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 91 percent / Et3N / tetrahydrofuran
2: 92 percent / NH2OH*HCl, Et3N, molecular sieves / tetrahydrofuran
3: 100 percent / NaBH3CN / acetic acid
4: 87 percent / Et3N / tetrahydrofuran
5: 92 percent / LiOH / methanol
6: 1) POCl3, pyridine / 1) THF, 2) THF
With
pyridine; lithium hydroxide; molecular sieve; hydroxylamine hydrochloride; sodium cyanoborohydride; triethylamine; trichlorophosphate;
In
tetrahydrofuran; methanol; acetic acid;
DOI:10.1016/0960-894X(96)00169-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 83 percent / TFA / CH2Cl2
2: 98 percent / 1-(3'-dimethylaminoproyl)-3-ethylcarbodiimide, 4-dimethylaminopyridine / CH2Cl2
3: 76 percent / TBAF / tetrahydrofuran
With
dmap; tetrabutyl ammonium fluoride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/0960-894X(96)00169-2
