C₁₄H₁₄O₄

Base Information

Chemical Name:C₁₄H₁₄O₄
CAS No.:1404100-74-8
Molecular Formula:C₁₄H₁₄O₄
Molecular Weight:246.263
Hs Code.:

C<sub>14</sub>H<sub>14</sub>O<sub>4</sub>

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Suppliers and Price of C₁₄H₁₄O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₄O₄

Chemical Property:

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Technology Process of C₁₄H₁₄O₄

There total 4 articles about C₁₄H₁₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 136041-03-7
C₁₄H₁₄O₄

: 1404100-74-8
C₁₄H₁₄O₄

Guidance literature:: With tungsten hexacarbonyl; triethylamine; In tetrahydrofuran; for 12h; Irradiation; Inert atmosphere;
DOI:10.1055/s-0032-1316536

Reference yield:

: 909797-76-8
1,3-dimethyl 2-benzyl-2-(prop-2-yn-1-yl)propanedioate

: 1404100-74-8
C₁₄H₁₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; methanol / 2.5 h / 20 °C

2: 3-wall resorcin[4]arene cavitand gold chloride complex / ⁽²⁾H₈-toluene / 24 h / 70 °C

With methanol; potassium hydroxide; In ⁽²⁾H₈-toluene;
DOI:10.1002/ejoc.201900829

Reference yield:

: 100-39-0
benzyl bromide

: 1404100-74-8
C₁₄H₁₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 20 °C

1.2: 2.5 h / 20 °C

2.1: caesium carbonate / toluene; acetone / Reflux

3.1: potassium hydroxide; methanol / 2.5 h / 20 °C

4.1: 3-wall resorcin[4]arene cavitand gold chloride complex / ⁽²⁾H₈-toluene / 24 h / 70 °C

With methanol; sodium hydride; caesium carbonate; potassium hydroxide; In tetrahydrofuran; ⁽²⁾H₈-toluene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201900829