Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3)

Base Information

Chemical Name:Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3)
CAS No.:350609-82-4
Molecular Formula:C₄₀H₆₇N₂ScSi
Molecular Weight:649.027
Hs Code.:

Sc(C<sub>3</sub>HN<sub>2</sub>(C<sub>4</sub>H<sub>9</sub>)2(C<sub>6</sub>H<sub>3</sub>(C<sub>3</sub>H<sub>7</sub>)2)2)(CH<sub>3</sub>)(CH<sub>2</sub>Si(CH<sub>3</sub>)3)

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Chemical Property of Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3)

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Technology Process of Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3)

There total 4 articles about Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 350609-81-3
Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)Cl

: 1822-00-0
trimethylsilylmethyllithium

: 350609-82-4
Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3)

Guidance literature:: In toluene; under Ar; toluene was vacuum-distd. into flask contg. Sc complex and LiCH2C(CH3)3; graduelly warmed to room temp.; stirred for 45 min; solvent removed (vac.); hexane added; mixt. filtered; vol. reduced; mixt. cooled to -78°C for 30 min; mixt. filtered; solvent removed (vac.); recrystd. (hexane);
DOI:10.1021/om010131o

Reference yield:

: 350609-70-0
Li(C₃H(C(CH₃)3)2(NC₆H₃(CH(CH₃)2)2)2)

: 350609-82-4
Sc(C₃HN₂(C₄H₉)2(C₆H₃(C₃H₇)2)2)(CH₃)(CH₂Si(CH₃)3)

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: toluene

3: B(C₆F₅)3

With B(C₆F₅)3; In toluene;
DOI:10.1021/om010131o