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boron 2-(4-dodecyloxybenzoyloxy)-1,3-benzoylmethanate difluoride

Base Information
  • Chemical Name:boron 2-(4-dodecyloxybenzoyloxy)-1,3-benzoylmethanate difluoride
  • CAS No.:1268325-85-4
  • Molecular Formula:C34H39BF2O5
  • Molecular Weight:576.488
  • Hs Code.:
boron 2-(4-dodecyloxybenzoyloxy)-1,3-benzoylmethanate difluoride

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Chemical Property of boron 2-(4-dodecyloxybenzoyloxy)-1,3-benzoylmethanate difluoride
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Technology Process of boron 2-(4-dodecyloxybenzoyloxy)-1,3-benzoylmethanate difluoride

There total 5 articles about boron 2-(4-dodecyloxybenzoyloxy)-1,3-benzoylmethanate difluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With boron trifluoride diethyl etherate; In toluene; Heating;
DOI:10.1134/S1070363210110150
Guidance literature:
In toluene; byproducts: HF; diketone and BF3*Et2O in toluene was heated with stirring; precipitated with cold (-40°C) Et2O, kept in liquid nitrogen, filtered, dried in vac., elem. anal.;
DOI:10.1134/S1070363210110150
Guidance literature:
Multi-step reaction with 3 steps
1: sodium hydroxide / ethanol; water / 0.17 h / Heating
2: ethanol; water / 7 h / Reflux
3: boron trifluoride diethyl etherate / toluene / Heating
With boron trifluoride diethyl etherate; sodium hydroxide; In ethanol; water; toluene;
DOI:10.1134/S1070363210110150
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