C₁₂₃⁽¹³⁾CH₁₇₅N₂O₁₉PS

Base Information

• Chemical Name: C₁₂₃⁽¹³⁾CH₁₇₅N₂O₁₉PS
• CAS No.: 247158-66-3
• Molecular Formula: C₁₂₄H₁₇₅N₂O₁₉PS
• Molecular Weight: 2061.78
• Mol file: 247158-66-3.mol

Synonyms:

Chemical Property of C₁₂₃⁽¹³⁾CH₁₇₅N₂O₁₉PS

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₁₂₃⁽¹³⁾CH₁₇₅N₂O₁₉PS

There total 1 articles about C₁₂₃⁽¹³⁾CH₁₇₅N₂O₁₉PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-3-benzyloxytetradecanoic acid (87357-67-3) + C81(13)CH111N2O15PS → C123(13)CH175N2O19PS (247158-66-3)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; WSCD-HCl; In chloroform; at 25 ℃; for 12h;

DOI:10.1246/bcsj.72.1857

Reference yield:

C123(13)CH175N2O19PS (247158-66-3) → C117(13)CH171N2O20P + C117(13)CH171N2O20P

Guidance literature:

With N-Bromosuccinimide; In water; acetone; at -30 ℃; for 2h; Title compound not separated from byproducts;

DOI:10.1246/bcsj.72.1857

Reference yield:

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate (990-91-0) + C123(13)CH175N2O19PS (247158-66-3) → C131(13)CH184N2O23P2

Guidance literature:

C₁₂₃⁽¹³⁾CH₁₇₅N₂O₁₉PS; With N-Bromosuccinimide; In water; acetone; at -30 ℃; for 2h;

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate; With lithium hexamethyldisilazane; In tetrahydrofuran; hexane; at -78 ℃; for 5h;

DOI:10.1246/bcsj.72.1857

upstream raw materials:

(R)-3-benzyloxytetradecanoic acid