C₂₂H₂₂FN₃O₃*ClH

Base Information

Chemical Name:C₂₂H₂₂FN₃O₃*ClH
CAS No.:1277100-06-7
Molecular Formula:C₂₂H₂₂FN₃O₃*ClH
Molecular Weight:431.894
Hs Code.:

C<sub>22</sub>H<sub>22</sub>FN<sub>3</sub>O<sub>3</sub>*ClH

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₂FN₃O₃*ClH

Chemical Property:

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Technology Process of C₂₂H₂₂FN₃O₃*ClH

There total 6 articles about C₂₂H₂₂FN₃O₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₀FN₃O₅

: 1277100-06-7
C₂₂H₂₂FN₃O₃*ClH

Guidance literature:: With hydrogenchloride; In chloroform; at 0 ℃; for 0.5h;
DOI:10.1016/j.ejps.2010.11.010

Reference yield:

: 1267329-49-6
3-(bromomethyl)-5-(4-fluorophenyl)-1,2-oxazole

: 1277100-06-7
C₂₂H₂₂FN₃O₃*ClH

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 4 h / 20 °C

2.1: hydrogenchloride / chloroform / 0.5 h / 0 °C

With hydrogenchloride; sodium hydride; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejps.2010.11.010

Reference yield:

: 31686-94-9
ethyl 4-(4-fluorophenyl)-2,4-dioxobutanoate

: 1277100-06-7
C₂₂H₂₂FN₃O₃*ClH

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydroxylamine hydrochloride / ethanol / 6 h / Reflux

2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 4 h / 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 24 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C

4.2: 4 h / 20 °C

5.1: hydrogenchloride / chloroform / 0.5 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; carbon tetrabromide; hydroxylamine hydrochloride; sodium hydride; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejps.2010.11.010