[iridium bis(7,8-benzoquinoline)(4,4-bis(2-phenylethyl)-2,2'-bipyridine)]hexafluorophosphate

Base Information

Chemical Name:[iridium bis(7,8-benzoquinoline)(4,4-bis(2-phenylethyl)-2,2'-bipyridine)]hexafluorophosphate
CAS No.:1343478-85-2
Molecular Formula:C₅₂H₄₀IrN₄*F₆P
Molecular Weight:1058.1
Hs Code.:

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Chemical Property of [iridium bis(7,8-benzoquinoline)(4,4-bis(2-phenylethyl)-2,2'-bipyridine)]hexafluorophosphate

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Technology Process of [iridium bis(7,8-benzoquinoline)(4,4-bis(2-phenylethyl)-2,2'-bipyridine)]hexafluorophosphate

There total 1 articles about [iridium bis(7,8-benzoquinoline)(4,4-bis(2-phenylethyl)-2,2'-bipyridine)]hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: ammonium hexafluorophosphate

: 52352-02-0
tetrakis-(benzo[h]quinoline(-1H))-μ-(dichloro)-diiridium(III)

: 1762-39-6
4,4′-diphenylethyl-2,2′-bipyridine

: 1343478-85-2
[iridium bis(7,8-benzoquinoline)(4,4-bis(2-phenylethyl)-2,2'-bipyridine)]hexafluorophosphate

Guidance literature:: In ethylene glycol; react. Ir complex with ligand in ethylene glycol under reflux at 150°C with stirring for 18 h, cooling to room temp., addn. of water, washing with Et2O, heating aq. layer at 70°C for 10 min, slow addn. of aq. NH4PF6; filtration, air drying of ppt. overnight, recrystn. (acetonitrile/Et2O vapor diffusion);
DOI:10.1016/j.poly.2011.08.010