C₄₂H₅₁N₄O₈PS

Base Information

Chemical Name:C₄₂H₅₁N₄O₈PS
CAS No.:1352230-16-0
Molecular Formula:C₄₂H₅₁N₄O₈PS
Molecular Weight:802.929
Hs Code.:

C<sub>42</sub>H<sub>51</sub>N<sub>4</sub>O<sub>8</sub>PS

Synonyms:

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Chemical Property of C₄₂H₅₁N₄O₈PS

Chemical Property:

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Technology Process of C₄₂H₅₁N₄O₈PS

There total 17 articles about C₄₂H₅₁N₄O₈PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 620630-82-2
1,2 5,6-O-di(isopropylidene)-α-D-allofuranose

: 1352230-16-0
C₄₂H₅₁N₄O₈PS

Guidance literature:: Multi-step reaction with 18 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 1 h / -78 - 20 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

7.2: 3 h / -78 °C

7.3: 20 °C

8.1: triethylamine / dmap / dichloromethane / 2.5 h / 0 °C

9.1: sulfuric acid / 16 h / 20 °C

10.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / Heating

10.2: Cooling with ice; Reflux

11.1: ammonia / methanol

13.1: pyridine / 16 h / 0 - 20 °C

14.1: potassium thioacetate / N,N-dimethyl-formamide / 20 °C

14.2: 2 h

15.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3 h

16.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 16 h / 20 °C

17.1: pyridine / 16 h / 0 - 20 °C

18.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; ammonia; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; dmap; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1352230-16-0
C₄₂H₅₁N₄O₈PS

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

4.2: 3 h / -78 °C

4.3: 20 °C

5.1: triethylamine / dmap / dichloromethane / 2.5 h / 0 °C

6.1: sulfuric acid / 16 h / 20 °C

7.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / Heating

7.2: Cooling with ice; Reflux

8.1: ammonia / methanol

10.1: pyridine / 16 h / 0 - 20 °C

11.1: potassium thioacetate / N,N-dimethyl-formamide / 20 °C

11.2: 2 h

12.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3 h

13.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 16 h / 20 °C

14.1: pyridine / 16 h / 0 - 20 °C

15.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; ammonia; water; dimethyl sulfoxide; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; dmap; sulfuric acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 956485-08-8
((3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1352230-16-0
C₄₂H₅₁N₄O₈PS

Guidance literature:: Multi-step reaction with 13 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

1.2: 1 h / -78 - 20 °C

2.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

2.2: 3 h / -78 °C

2.3: 20 °C

3.1: triethylamine / dmap / dichloromethane / 2.5 h / 0 °C

4.1: sulfuric acid / 16 h / 20 °C

5.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / Heating

5.2: Cooling with ice; Reflux

6.1: ammonia / methanol

8.1: pyridine / 16 h / 0 - 20 °C

9.1: potassium thioacetate / N,N-dimethyl-formamide / 20 °C

9.2: 2 h

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3 h

11.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 16 h / 20 °C

12.1: pyridine / 16 h / 0 - 20 °C

13.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; ammonia; water; dimethyl sulfoxide; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium thioacetate; dmap; sulfuric acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;