C₃CH₃NN(CCH₃NC₆H₃(CH(CH₃)2)2)2Co₂Cl₃(H₂O)2(CH₃CH₂OH)

Base Information

• Chemical Name: C₃CH₃NN(CCH₃NC₆H₃(CH(CH₃)2)2)2Co₂Cl₃(H₂O)2(CH₃CH₂OH)
• CAS No.: 1194302-96-9
• Molecular Formula: C₃₄H₅₃Cl₃Co₂N₄O₃
• Molecular Weight: 790.165
• Mol file: 1194302-96-9.mol

Synonyms:

Chemical Property of C₃CH₃NN(CCH₃NC₆H₃(CH(CH₃)2)2)2Co₂Cl₃(H₂O)2(CH₃CH₂OH)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃CH₃NN(CCH₃NC₆H₃(CH(CH₃)2)2)2Co₂Cl₃(H₂O)2(CH₃CH₂OH)

There total 1 articles about C₃CH₃NN(CCH₃NC₆H₃(CH(CH₃)2)2)2Co₂Cl₃(H₂O)2(CH₃CH₂OH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

ethanol (64-17-5) + HN2C3(CH3)(C(CH3)NC6H3(CH(CH3)2)2)2 (929260-74-2) + cobalt(II) chloride (7646-79-9,14543-09-0,16413-89-1) → C3CH3NN(CCH3NC6H3(CH(CH3)2)2)2Co2Cl3(H2O)2(CH3CH2OH) (1194302-96-9)

Guidance literature:

With KOC(CH₃)3; In tetrahydrofuran; (under N2); CoCl2 added to stirred soln. of ligand and KOC(CH3)3 in THF,stirred for 15 h at room temp.; evapd. to dryness, crystd. from CHCl3/EtOH or acetone; elem. anal.;

DOI:10.1039/b907817g

upstream raw materials:

ethanol

HN₂C₃(CH₃)(C(CH₃)NC₆H₃(CH(CH₃)2)2)2

cobalt(II) chloride