[MoCl₂(1,2-bis(diphenylphosphino)ethane)2]

Base Information

Chemical Name:[MoCl₂(1,2-bis(diphenylphosphino)ethane)2]
CAS No.:31096-73-8
Molecular Formula:C₅₂H₄₈Cl₂MoP₄
Molecular Weight:963.694
Hs Code.:

[MoCl<sub>2</sub>(1,2-bis(diphenylphosphino)ethane)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [MoCl₂(1,2-bis(diphenylphosphino)ethane)2]

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Technology Process of [MoCl₂(1,2-bis(diphenylphosphino)ethane)2]

There total 5 articles about [MoCl₂(1,2-bis(diphenylphosphino)ethane)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 50495-19-7,25145-64-6,41700-58-7
[Mo(N₂)2(1,2-bis(diphenylphosphino)ethane)2]

: 108-90-7
chlorobenzene

: 31096-73-8,59122-11-1,84413-89-8
[MoCl₂(1,2-bis(diphenylphosphino)ethane)2]

Guidance literature:: In chlorobenzene; byproducts: biphenyl, o-chlorobiphenyl, dihydro-o-chlorobiphenyl; Ar was bubbling through a soln. of complex in chlorobenzene for 5 h at 80°C and for 20 min at 132°C;; filtered, washed with n-hexane, dried in vac.; further organic productswere detected by gas-chromy. and mass-spectra;;
DOI:10.1016/S0022-328X(00)82474-2

Reference yield: 43.6%

: 100351-38-0
MoH(CHC(CH₃)C(O)OCH(CH₃)2)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

: 31096-73-8,59122-11-1,84413-89-8
[MoCl₂(1,2-bis(diphenylphosphino)ethane)2]

: 617-50-5
isopropyl isobutyrate

Guidance literature:: With hydrogenchloride; In hexane; Mo-complex dissolved in hexane was allowed to react in vacuo at room temp. for a day with HCl gas; ppt. was filtered off, washed with toluene, dried, analyzed as MoCl2(dppe)2, Me2CHCOO-i-Pr was detected in the filtrate by GLC analysis;