copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin

Base Information

Chemical Name:copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin
CAS No.:80529-85-7
Molecular Formula:C₆₄H₄₄N₄O₄Zn
Molecular Weight:998.468
Hs Code.:

Synonyms:

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Chemical Property of copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin

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Technology Process of copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin

There total 2 articles about copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: zinc p-anisylacetate

: 1074-82-4
potassium phtalimide

: 80529-85-7
copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin

: 14586-52-8
zinc(II) phthalocyanine

: 137164-81-9
meso-tri-p-anisyltetrabenzoporphinato zinc

: 137164-82-0
meso-mono-p-anisyltetrabenzoporphinato zinc

: meso-di-p-anisyltetrabenzoporphinato zinc

Guidance literature:: In solid; high temp. reaction, under N2; not isolated (FD-MS identification); contaminated with the corresponding p-methoxybenzyl adducts (FD-MS data);
DOI:10.1016/S0020-1693(00)87937-2

Reference yield:

: 55159-81-4
3-[(4-methoxyphenyl)methylidene]-2,3-dihydro-1H-isoindol-1-one

: 557-34-6
zinc diacetate

: 80529-85-7
copper meso-tetrakis(p-methoxyphenyl)tetrabenzoporphyrin

Guidance literature:: A mixt. of p-anisylidenenephthalimidine (ABI) and zinc acetate is heated at 360°C for 1h under N2.; Product ist washed with hot water and extd. with THF, evapn. gives a residue, which is chromd. first (Al2O3-column; dioxane), further purified by TLC on Al2O3 (solvent mixture of benzene/hexane/THF (10:10:1) used as an eluent), FD-MS analysis.;
DOI:10.1016/S0020-1693(00)85087-2