cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide

Base Information

Chemical Name:cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide
CAS No.:113579-89-8
Molecular Formula:C₁₃H₂₀N*I
Molecular Weight:317.213
Hs Code.:

Synonyms:

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Chemical Property of cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide

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Technology Process of cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide

There total 8 articles about cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3240-29-7
1-Phenylpent-4-en-1-one

: 113579-89-8,113579-90-1
cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide

Guidance literature:: Multi-step reaction with 5 steps

1: magnesium sulfate / diethyl ether / 70 - 80 °C / autoclave

2: sodium borohydride (NaBH₄) / methanol / Ambient temperature

3: butyllithium / tetrahydrofuran / 0.5 h / -10 °C

4: 0.25M lithium perchlorate / tetrahydrofuran; hexamethylphosphoric acid triamide / -10 °C / anodic oxidation

5: 62 mg / diethyl ether / 2 h / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; lithium perchlorate; magnesium sulfate; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1016/S0040-4020(01)89956-7

Reference yield:

: 102632-99-5,134679-60-0,144178-31-4,54525-86-9
1-phenyl-4-penten-1-ol

: 113579-89-8,113579-90-1
cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3 h / Heating

2: magnesium sulfate / diethyl ether / 70 - 80 °C / autoclave

3: sodium borohydride (NaBH₄) / methanol / Ambient temperature

4: butyllithium / tetrahydrofuran / 0.5 h / -10 °C

5: 0.25M lithium perchlorate / tetrahydrofuran; hexamethylphosphoric acid triamide / -10 °C / anodic oxidation

6: 62 mg / diethyl ether / 2 h / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; lithium perchlorate; magnesium sulfate; pyridinium chlorochromate; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)89956-7

Reference yield:

: 104886-43-3
N-methyl-1-phenylpent-4-en-1-amine

: 113579-89-8,113579-90-1
cis-1,1,2-trimethyl-5-phenylpyrrolidinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: butyllithium / tetrahydrofuran / 0.5 h / -10 °C

2: 0.25M lithium perchlorate / tetrahydrofuran; hexamethylphosphoric acid triamide / -10 °C / anodic oxidation

3: 62 mg / diethyl ether / 2 h / Ambient temperature

With n-butyllithium; lithium perchlorate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1016/S0040-4020(01)89956-7