((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2

Base Information

Chemical Name:((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2
CAS No.:121030-85-1
Molecular Formula:CH₂Cl₂*C₆₂H₅₈Cl₂N₂O₁₀P₂Rh₄
Molecular Weight:1620.56
Hs Code.:

((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2

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Chemical Property of ((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2

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Technology Process of ((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2

There total 1 articles about ((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119326-23-7
((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 121030-85-1
((η5-cyclopentadienyl)rhodium(μ-diethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2

Guidance literature:: With CH₂Cl₂; In dichloromethane; Treating a soln. of Rh-complex with DEA, stirring for ca 2 h.; Reducing volume of solvent, pptg. by addn. of n-hexane, filtration, washing (Et2O), drying, recrystn. (CH2Cl2/Et2O), elem. anal.;