((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

Base Information

Chemical Name:((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)
CAS No.:119326-23-7
Molecular Formula:C₂₄H₁₉ClNO₂PRh₂
Molecular Weight:625.658
Hs Code.:

Synonyms:((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

Suppliers and Price of ((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

There total 1 articles about ((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: di(rhodium)tetracarbonyl dichloride

: 119326-22-6
{Rh(η5-C5H5)(CO)(Ph2PPy)}

: 119326-23-7
{(η5-C5H5)Rh(μ-CO)(μ-Ph2PPy)Rh(CO)Cl}

Guidance literature:: In dichloromethane; soln. stirred (ca. 1 h, N2); diethyl ether-hexane (1:2) added; elem. anal.;

Reference yield: 94.0%

: 119326-23-7
{(η5-C5H5)Rh(μ-CO)(μ-Ph2PPy)Rh(CO)Cl}

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

: 119336-07-1
{(η5-C5H5)Rh(μ-Ph2PPy)(μ-SO2)Rh(CO)Cl}

Guidance literature:: In diethyl ether; SO2 bubbled into soln. of complex (N2); solvent removed from ppt. by syringe, recrystd. from dichloromethane-hexane (1:3); elem. anal.;

Reference yield: 92.0%

: 119326-23-7
((η5-cyclopentadienyl)rhodium(μ-carbonyl)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)Cl)

: 762-42-5
dimethyl acetylenedicarboxylate

: 121072-51-3
((η5-cyclopentadienyl)rhodium(μ-dimethyl acetylenedicarboxylate)(μ-2-(diphenylphosphino)pyridine)rhodium(carbonyl)(μ-Cl))2*CH2Cl2

Guidance literature:: With CH₂Cl₂; In dichloromethane; Treating a soln. of Rh-complex with DMA, stirring for ca. 2 h.; Reducing volume of solvent, pptg. by addn. of n-hexane, filtration, washing (Et2O), drying, recrystn. (CH2Cl2/Et2O), elem. anal.;