methyl(η5-indenyl)bis(triphenylphosphine)iridium(III) tetrafluoroborate

Base Information

Chemical Name:methyl(η5-indenyl)bis(triphenylphosphine)iridium(III) tetrafluoroborate
CAS No.:119793-89-4
Molecular Formula:BF₄*CH₂Cl₂*C₄₆H₄₀IrP₂
Molecular Weight:1018.73
Hs Code.:

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Chemical Property of methyl(η5-indenyl)bis(triphenylphosphine)iridium(III) tetrafluoroborate

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Technology Process of methyl(η5-indenyl)bis(triphenylphosphine)iridium(III) tetrafluoroborate

There total 1 articles about methyl(η5-indenyl)bis(triphenylphosphine)iridium(III) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13755-29-8
sodium tetrafluoroborate

: (η(5)-indenyl)Ir(PPh3)2

: 74-88-4
methyl iodide

: 119793-89-4
methyl(η5-indenyl)bis(triphenylphosphine)iridium(III) tetrafluoroborate

Guidance literature:: In tetrahydrofuran; treating (Ind)IrL2 in THF with MeI (-78°C), warming to 20°C, stirring (dark, 1 h), adding excess NaBF4; adding Et2O, pptn., recrystn. (CH2Cl2/Et2O); elem. anal.;
DOI:10.1021/om00107a016