Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Base Information

Chemical Name:Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester
CAS No.:146667-77-8
Molecular Formula:C₃₈H₆₅O₉PSi
Molecular Weight:724.988
Hs Code.:

Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

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Chemical Property of Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

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Technology Process of Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

There total 3 articles about Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphorous acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

: 146667-77-8
Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Guidance literature:: With dihydrogen peroxide; Yield given;
DOI:10.1016/0040-4039(93)88016-C

Reference yield:

: 41662-46-8
Bis(allyl)monochlorophosphit

: 146667-77-8
Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, DMAP / 1.5 h / 25 °C

2: 30percent H₂O₂

With pyridine; dmap; dihydrogen peroxide;
DOI:10.1016/0040-4039(93)88016-C

Reference yield:

: 146667-76-7
(2R,3S,5S,7R,8S,9S)-7-(2-Benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]decan-3-ol

: 146667-77-8
Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, DMAP / 1.5 h / 25 °C

2: 30percent H₂O₂

With pyridine; dmap; dihydrogen peroxide;
DOI:10.1016/0040-4039(93)88016-C