Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Base Information

Chemical Name:Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester
CAS No.:146667-78-9
Molecular Formula:C₃₅H₆₁O₉PSi
Molecular Weight:684.923
Hs Code.:

Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

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Chemical Property of Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

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Technology Process of Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

There total 3 articles about Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146667-77-8
Phosphoric acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

: 146667-78-9
Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Guidance literature:: With Pd(Ph₃P); N-butylamine; triphenylphosphine; In tetrahydrofuran; at 50 ℃; for 48h;
DOI:10.1016/0040-4039(93)88016-C

Reference yield:

: 146667-76-7
(2R,3S,5S,7R,8S,9S)-7-(2-Benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]decan-3-ol

: 146667-78-9
Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine, DMAP / 1.5 h / 25 °C

2: 30percent H₂O₂

3: n-BuNH₂, Ph₃P, Pd(Ph₃P) / tetrahydrofuran / 48 h / 50 °C

With pyridine; dmap; Pd(Ph₃P); dihydrogen peroxide; N-butylamine; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/0040-4039(93)88016-C

Reference yield:

: Phosphorous acid diallyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

: 146667-78-9
Phosphoric acid allyl ester (2S,3S,5S,7R,8S,9S)-7-(2-benzyloxy-ethyl)-2-((R)-1-methoxy-ethyl)-4,4,8-trimethyl-9-triisopropylsilanyloxy-1,6-dioxa-spiro[4.5]dec-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30percent H₂O₂

2: n-BuNH₂, Ph₃P, Pd(Ph₃P) / tetrahydrofuran / 48 h / 50 °C

With Pd(Ph₃P); dihydrogen peroxide; N-butylamine; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/0040-4039(93)88016-C