Ti(((C₆H₅)2PCH₂)2)Cl₂((CH₃)3CS)2

Base Information

Chemical Name:Ti(((C₆H₅)2PCH₂)2)Cl₂((CH₃)3CS)2
CAS No.:91709-20-5
Molecular Formula:C₃₄H₄₂Cl₂P₂S₂Ti
Molecular Weight:695.573
Hs Code.:

Ti(((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)2)Cl<sub>2</sub>((CH<sub>3</sub>)3CS)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ti(((C₆H₅)2PCH₂)2)Cl₂((CH₃)3CS)2

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Technology Process of Ti(((C₆H₅)2PCH₂)2)Cl₂((CH₃)3CS)2

There total 1 articles about Ti(((C₆H₅)2PCH₂)2)Cl₂((CH₃)3CS)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 16203-42-2
lithium tert-butylsulfide

: 7550-45-0
titanium tetrachloride

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 91709-20-5
Ti(((C₆H₅)2PCH₂)2)Cl₂((CH₃)3CS)2

Guidance literature:: In tetrahydrofuran; benzene; TiCl4 adding to a ligand soln. in hexane at -78°C in inert atm.,stirring for 0.5 h at -78°C, THF soln. of Li deriv. adding dropwise, allowing to warm to room temp. over 5 h, volatiles removing in vacuo, residue extg. with hexane, concg.; isolated by cooling hexane soln. at -25°C for 12 h; identified by elem. anal., IR and NMR spectra;
DOI:10.1016/S0277-5387(00)84527-1