2-hydroxy-3,4,5,6-tetramethoxy propiophenone

Base Information

Chemical Name:2-hydroxy-3,4,5,6-tetramethoxy propiophenone
CAS No.:117970-66-8
Molecular Formula:C₁₃H₁₈O₆
Molecular Weight:270.282
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-3,4,5,6-tetramethoxy propiophenone

Chemical Property:

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Technology Process of 2-hydroxy-3,4,5,6-tetramethoxy propiophenone

There total 6 articles about 2-hydroxy-3,4,5,6-tetramethoxy propiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 119232-80-3
2,5-dihydroxy-3,4,6-trimethoxypropiophenone

: 77-78-1
dimethyl sulfate

: 117970-66-8
2-hydroxy-3,4,5,6-tetramethoxy propiophenone

Guidance literature:: With potassium carbonate; In benzene;
DOI:10.1016/S0040-4039(00)86056-6

Reference yield:

: 21450-56-6
1,2,3,4-tetramethoxybenzene

: 117970-66-8
2-hydroxy-3,4,5,6-tetramethoxy propiophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / POCl₃

2: 1.) mCPBA; 2.) aq. KOH 10percent / 1.) CH₂Cl₂, rt; 2.) MeOH

3: 92 percent / acetone

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In acetone;
DOI:10.1016/S0040-4039(00)80196-3

Reference yield:

: 65884-12-0
2,3,4,5-tetramethoxybenzaldehyde

: 117970-66-8
2-hydroxy-3,4,5,6-tetramethoxy propiophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) mCPBA; 2.) aq. KOH 10percent / 1.) CH₂Cl₂, rt; 2.) MeOH

2: 92 percent / acetone

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In acetone;
DOI:10.1016/S0040-4039(00)80196-3