chloronickel(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene

Base Information

• Chemical Name: chloronickel(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene
• CAS No.: 689262-19-9
• Molecular Formula: C₅₈H₃₈ClN₅NiO₄
• Molecular Weight: 963.114

Synonyms:

Chemical Property of chloronickel(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene

Chemical Property:

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Technology Process of chloronickel(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene

There total 1 articles about chloronickel(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6,6,21,21-tetraphenyl-11,16-bis(4-nitrophenyl)-meta-benziporphodimethene + nickel dichloride (83864-14-6) → chloronickel(II) 11,16-bis(4-nitrophenyl)-6,6,21,21-tetraphenyl-meta-benziporphodimethene (689262-19-9)

Guidance literature:

In chloroform; acetonitrile; a mixt. of the ligand and NiCl2 was refluxed in CHCl3-MeCN for 6 h, the progress of the reaction can be monitored by UV-vis spectroscopy; evapd., remaining MeCN was removed by repeated adding small portions of CH2Cj2 to the residue and evaporating, the residue was dissolved in CH2Cl2, filtd., evapd., recrystd. from hexane;

DOI:10.1021/ja039384u

upstream raw materials:

nickel dichloride

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