5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N¹,N¹-dimethylamidino>-4-methyl-1,2,3-triazol

Base Information

• Chemical Name: 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N¹,N¹-dimethylamidino>-4-methyl-1,2,3-triazol
• CAS No.: 84275-00-3
• Molecular Formula: C₁₇H₂₆N₆O₃S
• Molecular Weight: 394.498

Synonyms:

Chemical Property of 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N¹,N¹-dimethylamidino>-4-methyl-1,2,3-triazol

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N¹,N¹-dimethylamidino>-4-methyl-1,2,3-triazol

There total 4 articles about 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N¹,N¹-dimethylamidino>-4-methyl-1,2,3-triazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N--4-methoxybenzolsulfonamid (84274-74-8) + methyl(diethylamino)acetylene (4231-35-0) → 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N1,N1-dimethylamidino>-4-methyl-1,2,3-triazol (84275-00-3)

Guidance literature:

In chloroform; for 48h; Ambient temperature;

Reference yield:

4-methoxybenzene sulfonamide (1129-26-6) → 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N1,N1-dimethylamidino>-4-methyl-1,2,3-triazol (84275-00-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 92 percent / benzene / 2 h / Heating

2: 75 percent / N₂H₄*H₂O / ethanol / 1 h / Ambient temperature

3: 46 percent / isoamylnitrite / CHCl₃; acetic acid / 2 h / Ambient temperature

4: 78 percent / CHCl₃ / 48 h / Ambient temperature

With hydrazine hydrate; isopentyl nitrite; In ethanol; chloroform; acetic acid; benzene;

Reference yield:

N--4-methoxybenzolsulfonamid (84302-52-3) → 5-Diethylamino-1-2-(4-methoxyphenylsulfonyl)-N1,N1-dimethylamidino>-4-methyl-1,2,3-triazol (84275-00-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 75 percent / N₂H₄*H₂O / ethanol / 1 h / Ambient temperature

2: 46 percent / isoamylnitrite / CHCl₃; acetic acid / 2 h / Ambient temperature

3: 78 percent / CHCl₃ / 48 h / Ambient temperature

With hydrazine hydrate; isopentyl nitrite; In ethanol; chloroform; acetic acid;

upstream raw materials:

N--4-methoxybenzolsulfonamid

methyl(diethylamino)acetylene

4-methoxybenzene sulfonamide

N--4-methoxybenzolsulfonamid

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