2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene

Base Information

• Chemical Name: 2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene
• CAS No.: 1174274-70-4
• Molecular Formula: C₂₈H₂₇FeNO
• Molecular Weight: 449.375
• Mol file: 1174274-70-4.mol

Synonyms:

Chemical Property of 2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene

There total 1 articles about 2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-ferrocenyl-1-(4-aminophenyl)-1-phenyl-but-1-ene (1046455-84-8,1148109-22-1,1046322-67-1) + acetyl chloride (75-36-5) → 2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene (1174274-70-4,1148109-03-8)

Guidance literature:

With pyridine; In tetrahydrofuran; pyridine; (Ar); std. Schlenk technique; CH3COCl and pyridine were added to soln. of Fe complex in THF; stirred for 3 h; H2O added; extd. (CH2Cl2); org. phase washed (H2O); dried (MgSO4); filtered; evapd.; chromd. (silica gel, ether/pentane, 1/1);

DOI:10.1016/j.jorganchem.2008.11.035

Reference yield:

2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene (1174274-70-4,1148109-03-8) → 2-ferrocenyl-1-(4-acetylaminophenyl)-1-phenyl-but-1-ene

Guidance literature:

In diethyl ether; pentane; (Ar); std. Schlenk technique; Fe complex was recrystd. from ether/pentane; elem. anal.;

DOI:10.1016/j.jorganchem.2008.11.035

upstream raw materials:

2-ferrocenyl-1-(4-aminophenyl)-1-phenyl-but-1-ene

acetyl chloride