L-Proline, 1-[N-[1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl]-L-alanyl]-, 1,1-dimethylethyl ester, monohydrochloride

Base Information

Chemical Name:L-Proline, 1-[N-[1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl]-L-alanyl]-, 1,1-dimethylethyl ester, monohydrochloride
CAS No.:105499-26-1
Molecular Formula:C₂₄H₃₆N₂O₆*ClH
Molecular Weight:485.021
Hs Code.:
Mol file:105499-26-1.mol

Synonyms:

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Chemical Property of L-Proline, 1-[N-[1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl]-L-alanyl]-, 1,1-dimethylethyl ester, monohydrochloride

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Technology Process of L-Proline, 1-[N-[1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl]-L-alanyl]-, 1,1-dimethylethyl ester, monohydrochloride

There total 2 articles about L-Proline, 1-[N-[1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl]-L-alanyl]-, 1,1-dimethylethyl ester, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122442-04-0
(1S)-N-<1-(ethoxycarbonyl)-3-oxo-3-phenylpropyl>-(S)-alanyl-(S)-proline tert-butyl ester hydrochloride

: 105499-26-1,105499-31-8,105560-98-3
(1S)-N-<1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl>-(S)-alanyl-(S)-proline tert-butyl ester hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; Ambient temperature;

Reference yield:

: 29375-30-2
(S)-alanyl-(S)-proline tert-butyl ester

: 105499-26-1,105499-31-8,105560-98-3
(1S)-N-<1-(ethoxycarbonyl)-3-hydroxy-3-phenylpropyl>-(S)-alanyl-(S)-proline tert-butyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / 2.) 3 N HCl / ethyl acetate / 2 h / 0 °C

2: H₂ / 10percent Pd on charcoal / ethanol / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate;