decafluorocyclohexylidenimine

Base Information

Chemical Name:decafluorocyclohexylidenimine
CAS No.:74528-69-1
Molecular Formula:C₆HF₁₀N
Molecular Weight:277.065
Hs Code.:

Synonyms:

Suppliers and Price of decafluorocyclohexylidenimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of decafluorocyclohexylidenimine

Chemical Property:

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Technology Process of decafluorocyclohexylidenimine

There total 3 articles about decafluorocyclohexylidenimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5927-67-3
decafluoro-1,2-epoxycyclohexane

: 74528-69-1
decafluorocyclohexylidenimine

Guidance literature:: Multi-step reaction with 2 steps

1: 139 g / KF / tetrahydrothiophene 1,1-dioxide / 5.5 h / 140 - 185 °C

2: 1.) pyridine; 2.) NH₃; 3.) POCl₃ / 3.) 90-100 deg C, 1h

With pyridine; potassium fluoride; ammonia; trichlorophosphate; In sulfolane;
DOI:10.1016/S0022-1139(00)81469-4

Reference yield:

: 355-75-9
decafluorocyclohex-1-ene

: 74528-69-1
decafluorocyclohexylidenimine

Guidance literature:: Multi-step reaction with 3 steps

1: 190.2 g / H₂O₂, KOH / methanol / 3.5 h / -15 deg C to room temp.

2: 139 g / KF / tetrahydrothiophene 1,1-dioxide / 5.5 h / 140 - 185 °C

3: 1.) pyridine; 2.) NH₃; 3.) POCl₃ / 3.) 90-100 deg C, 1h

With pyridine; potassium fluoride; potassium hydroxide; ammonia; dihydrogen peroxide; trichlorophosphate; In sulfolane; methanol;
DOI:10.1016/S0022-1139(00)81469-4

Reference yield:

: 1898-91-5
perfluorocyclohexanone

: 74528-69-1
decafluorocyclohexylidenimine

Guidance literature:: With pyridine; ammonia; trichlorophosphate; Yield given. Multistep reaction; 3.) 90-100 deg C, 1h;
DOI:10.1016/S0022-1139(00)81469-4