Technology Process of C29H42O5S2Sn
There total 6 articles about C29H42O5S2Sn which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N,N-dimethylglycine hydrochoride; caesium carbonate / copper(l) iodide / 1,4-dioxane / 22 h / 90 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 192 h / 0 - 20 °C
3: thiourea / methanol; dichloromethane / 20 °C
4: toluene / 12 h / 80 °C
With
N,N-dimethylglycine hydrochoride; caesium carbonate; thiourea; 3-chloro-benzenecarboperoxoic acid;
copper(l) iodide;
In
1,4-dioxane; methanol; dichloromethane; toluene;
1: Ullmann Coupling / 4: Mascaretti;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N,N-dimethylglycine hydrochoride; caesium carbonate / copper(l) iodide / 1,4-dioxane / 22 h / 90 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 192 h / 0 - 20 °C
3: thiourea / methanol; dichloromethane / 20 °C
4: toluene / 12 h / 80 °C
With
N,N-dimethylglycine hydrochoride; caesium carbonate; thiourea; 3-chloro-benzenecarboperoxoic acid;
copper(l) iodide;
In
1,4-dioxane; methanol; dichloromethane; toluene;
1: Ullmann Coupling / 4: Mascaretti;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C
2: N,N-dimethylglycine hydrochoride; caesium carbonate / copper(l) iodide / 1,4-dioxane / 22 h / 90 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 192 h / 0 - 20 °C
4: thiourea / methanol; dichloromethane / 20 °C
5: toluene / 12 h / 80 °C
With
N,N-dimethylglycine hydrochoride; potassium carbonate; caesium carbonate; thiourea; 3-chloro-benzenecarboperoxoic acid;
copper(l) iodide;
In
1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
2: Ullmann Coupling / 5: Mascaretti;