[Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2

Base Information

Chemical Name:[Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2
CAS No.:1416162-95-2
Molecular Formula:C₄₂H₅₄N₂O₄Pd₂Si₂
Molecular Weight:919.913
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2

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Technology Process of [Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2

There total 1 articles about [Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1416162-94-1
[Pd{CH₂SiPh₂(CH₂NC₅H₁₀)-κ²C,N}(NCMe)₂]BF₄

: 127-08-2
potassium acetate

: 1416162-95-2
[Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2

Guidance literature:: In tetrahydrofuran; acetonitrile; byproducts: KBF4, CH3CN; under oxygen-free dried N2, stirred at room temp. for 1 h; evapd. to dryness, yielding dark residue, extd. with toluene, yellow soln. concd. to dryness, solid washed with hexane, dried in vac., detd. by 1H NMR, 13C NMR, IR, elem. anal.;
DOI:10.1002/ejic.201200257

Reference yield: 23.0%

: [Pd(CH2SiPh2(CH2NC5H10)-κ2C,N)(μ-dmpz-κN:κ'N)]2

: 1416162-95-2
[Pd(CH2SPh2(CH2NC5H10)-κ2C,N)(μ-O2CCH3-κO:κ'O)]2

: 1416162-98-5
[Pd2(CH2SiPh2(CH2NC5H10)-κ2C,N)2(μ-O2CCH3-κO:κ'O)(μ-dmpz-κN:κ'N)]

Guidance literature:: In dichloromethane; under oxygen-free dried N2, heated in closed Schlenk flask at 40°C for 24 h; soln. filtered, hexane added to resulting yellow soln., concd. in vac., cooled at -20°C, sturting materials collected, mother liquor concd., pale yellow crystals washed with hexane, dried in vac., detd. by 1H NMR, IR, elem. anal.;
DOI:10.1002/ejic.201200257