((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃

Base Information

Chemical Name:((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃
CAS No.:80611-31-0
Molecular Formula:C₁₂H₁₈FeO₂Si
Molecular Weight:278.206
Hs Code.:

((CH<sub>3</sub>)3SiC<sub>5</sub>H<sub>4</sub>)Fe(CO)2CH<sub>2</sub>CH<sub>3</sub>

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Chemical Property of ((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃

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Technology Process of ((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃

There total 1 articles about ((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74-96-4
ethyl bromide

: 41680-29-9
FpSiMe₂Ph

: (η5-C5H4Me)Fe(CO)2(SiMe3)

: 80611-31-0
((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃

: 97279-51-1
((CH₃)3SiC₅H₃CH₃)Fe(CO)2C₂H₅

: 97279-52-2
((CH₃)3SiC₅H₃CH₃)Fe(CO)2C₂H₅

: 97279-57-7
(C₆H₅(CH₃)2SiC₅H₄)Fe(CO)2CH₂CH₃

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; under N2, soln. of Fe complexes (1:1 molar ratio) in THF at -78°C treated with soln. of n-BuLi in hexane, stirred at -78°C for 4 h, warmed to 0°C during 1 h, EtBr added, stirred for 2 h at 0°C; evapd. in vac., chromd. (Florisil, petroleum ether), evapd.;
DOI:10.1021/om00128a004

Reference yield:

: 80611-31-0
((CH₃)3SiC₅H₄)Fe(CO)2CH₂CH₃

: (CH₃)3SiC₅H₄Fe(CO)(P(C₆H₅)3)COC₂H₅

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; to THF soln. added PPh3 in 20 % excess at 70°C for 72 h; elem. anal.;
DOI:10.1016/S0022-328X(00)89048-8