Technology Process of C31H45N3O3S
There total 7 articles about C31H45N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium aluminium tetrahydride / diethyl ether / -10 °C
2: Dess-Martin periodane / dichloromethane / 20 °C
3: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C
4: trifluoroacetic acid / 20 °C
5: sodium tris(acetoxy)borohydride
With
lithium aluminium tetrahydride; sodium tris(acetoxy)borohydride; Dess-Martin periodane; trifluoroacetic acid;
In
diethyl ether; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.117
- Guidance literature:
-
Multi-step reaction with 6 steps
1: palladium on carbon; hydrogen / ethanol
2: lithium aluminium tetrahydride / diethyl ether / -10 °C
3: Dess-Martin periodane / dichloromethane / 20 °C
4: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C
5: trifluoroacetic acid / 20 °C
6: sodium tris(acetoxy)borohydride
With
lithium aluminium tetrahydride; palladium on carbon; hydrogen; sodium tris(acetoxy)borohydride; Dess-Martin periodane; trifluoroacetic acid;
In
diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.12.117
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C
2: trifluoroacetic acid / 20 °C
3: sodium tris(acetoxy)borohydride
With
sodium tris(acetoxy)borohydride; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.bmcl.2011.12.117