((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl

Base Information

Chemical Name:((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl
CAS No.:477291-20-6
Molecular Formula:C₂₄H₄₅ClP₃Rh
Molecular Weight:564.901
Hs Code.:

((i)Pr<sub>2</sub>P(CH<sub>2</sub>)3P(Ph)(CH<sub>2</sub>)3P(i)Pr)RhCl

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Chemical Property of ((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl

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Technology Process of ((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl

There total 1 articles about ((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 477291-36-4
((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhSi(SEt)3

: 477291-20-6
((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl

Guidance literature:: In 1,4-dioxane; benzene-d6; byproducts: HSi(SEt)3; under N2; Rh-contg. compd. (0.012 mmol) was dissolved in C6D6 and treated with an equiv. amt. of HCl soln. in 1,4-dioxane; NMR spectra;
DOI:10.1021/om020120a

Reference yield: 88.0%

: 477291-20-6
((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl

: 594-19-4
tert.-butyl lithium

: 477291-24-0
((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhH

Guidance literature:: In tetrahydrofuran; pentane; byproducts: CH2CMe2; under N2; a soln. of Rh-contg. compd. (0.2 mmol) in THF was treated with(t)BuLi (0.2 mmol) in pentane at -30°C; warming to room temp.; t he mixt. stood at room temp. for 2 h; the solvents were evapd. in vac., the residue was redissolved in pentane, and the soln. filtered; the filtrate was evapd. and dried in vac.; NMRstudies;
DOI:10.1021/om020120a

Reference yield: 85.0%

: 477291-20-6
((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhCl

: 917-54-4
methyllithium

: 477291-28-4
((i)Pr₂P(CH₂)3P(Ph)(CH₂)3P(i)Pr)RhMe

Guidance literature:: In tetrahydrofuran; diethyl ether; under N2; a soln. of Rh-contg. compd. (0.3 mmol) in THF was treated withMeLi (0.3 mmol) in ether at -30°C; warming to room temp.; the mi xt. stood at room temp. for 2 h; the solvents were evapd. in vac., the residue was dissolved in pentane, and the soln. filtered; the filtrate was evapd. and dried in vac.; elem.anal.;
DOI:10.1021/om020120a