C₁₃H₁₃FN₂O₂

Base Information

Chemical Name:C₁₃H₁₃FN₂O₂
CAS No.:1384167-22-9
Molecular Formula:C₁₃H₁₃FN₂O₂
Molecular Weight:248.257
Hs Code.:

C<sub>13</sub>H<sub>13</sub>FN<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₃FN₂O₂

Chemical Property:

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Technology Process of C₁₃H₁₃FN₂O₂

There total 3 articles about C₁₃H₁₃FN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₇FN₂O₂

: 1384167-22-9
C₁₃H₁₃FN₂O₂

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 12h;
DOI:10.1016/j.bmcl.2012.05.020

Reference yield:

: 1341198-43-3
1-benzyl-4-iodo-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

: 1384167-22-9
C₁₃H₁₃FN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / 15 h / 90 °C

2: formic acid; ammonium formate; palladium(II) hydroxide / 6 h / 60 °C

3: water; sodium hydroxide / tetrahydrofuran; ethanol / 12 h / 50 °C

With formic acid; water; ammonium formate; palladium diacetate; palladium(II) hydroxide; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2012.05.020

Reference yield:

: 615-79-2
ethyl 2,4-diketopentanoate

: 1384167-22-9
C₁₃H₁₃FN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: hydrazine hydrochloride / ethanol; water / 1 h / 60 °C

2: ammonium cerium (IV) nitrate; iodine / acetonitrile / 4 h / 20 °C

3: sodium hydride / tetrahydrofuran / 6 h / 0 - 20 °C

4: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / 15 h / 90 °C

5: formic acid; ammonium formate; palladium(II) hydroxide / 6 h / 60 °C

6: water; sodium hydroxide / tetrahydrofuran; ethanol / 12 h / 50 °C

With formic acid; ammonium cerium (IV) nitrate; hydrazine hydrochloride; water; iodine; ammonium formate; palladium diacetate; palladium(II) hydroxide; sodium hydride; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In tetrahydrofuran; ethanol; water; acetonitrile;
DOI:10.1016/j.bmcl.2012.05.020