Technology Process of C29H29NO8S
There total 11 articles about C29H29NO8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere
1.2: 145 °C / Inert atmosphere
2.1: potassium hydroxide / water / 4 h / Inert atmosphere; Reflux
3.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere
4.1: boron tribromide / dichloromethane / 4 h / 20 °C
4.2: 16 h / 0 - 20 °C
5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
6.1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid
7.1: hydrogenchloride / water / 3 h / Reflux; Inert atmosphere
With
pyridine; hydrogenchloride; 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; boron tribromide; sodium hydride; p-toluenesulfonyl chloride; triphenylphosphine; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
5.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid
2: hydrogenchloride / water / 3 h / Reflux; Inert atmosphere
With
hydrogenchloride; 2,6-di-tert-butyl-pyridine;
In
water;
DOI:10.1039/c2ob00022a
- Guidance literature:
-
With
hydrogenchloride;
In
water;
for 3h;
Reflux;
Inert atmosphere;
DOI:10.1039/c2ob00022a
