{(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}

Base Information

Chemical Name:{(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}
CAS No.:135973-15-8
Molecular Formula:C₂₅H₂₆Cl₃NPPdRh
Molecular Weight:687.146
Hs Code.:

Synonyms:

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Chemical Property of {(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}

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Technology Process of {(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}

There total 2 articles about {(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 135973-06-7
chlorocycloocta-1,5-diene(diphenyl-2-pyridylphosphine)rhodium(I)

: 135973-15-8
{(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}

Guidance literature:: In dichloromethane; (N2), added dropwise to stirred soln. of the Rh-complex, after 15 min. volume reduced, added petroleum ether; filtered, washed with diethyl ether, dried in vac.; elem. anal.;

Reference yield: 95.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 37943-90-1
2-(diphenylphosphino)pyridine

: 135973-15-8
{(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}

Guidance literature:: In dichloromethane; (N2), Ph2PPy added to a soln. of Pd-complex, subsequent addn. of Rh-complex to the mixture, reduced volume, added diethyl ether; filtered, washed with diethyl ether, dried in vac.; elem. anal.;

Reference yield:

: 135973-15-8
{(cycloocta-1,5-diene)Rh(μ-Cl)(μ-2(diphenylphosphino)pyridine)PdCl2}

: 119072-55-8,7188-38-7
tert-butylisonitrile

: {(tert-BuNC)2Cl2Rh(μ-2-(diphenylphosphino)pyridine)Pd(μ-Cl)}2

Guidance literature:: In dichloromethane; (N2), added dropwise, added petroleum ether; filtered, washed with diethyl ether, dried in vac.; elem. anal., IR;