Pyridazine, 6-chloro-3-methyl-4-phenyl-

Base Information

Chemical Name:Pyridazine, 6-chloro-3-methyl-4-phenyl-
CAS No.:105538-79-2
Molecular Formula:C11H9ClN2
Molecular Weight:204.659
Hs Code.:
European Community (EC) Number:835-184-9
DSSTox Substance ID:DTXSID801291737
Mol file:105538-79-2.mol

Synonyms:Pyridazine, 6-chloro-3-methyl-4-phenyl-;105538-79-2;6-CHLORO-3-METHYL-4-PHENYLPYRIDAZINE;SCHEMBL25230310;DTXSID801291737;AT11131;EN300-3495592;Z1079105390

Suppliers and Price of Pyridazine, 6-chloro-3-methyl-4-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Pyridazine, 6-chloro-3-methyl-4-phenyl-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:204.0454260
Heavy Atom Count:14
Complexity:180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN=C(C=C1C2=CC=CC=C2)Cl

Technology Process of Pyridazine, 6-chloro-3-methyl-4-phenyl-

There total 3 articles about Pyridazine, 6-chloro-3-methyl-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 68240-43-7
4,6-dichloro-3-methylpyridazine

: 98-80-6
phenylboronic acid

: 1416371-83-9
C₁₁H₉ClN₂

: 105538-79-2
6-Chloro-3-methyl-4-phenyl-pyridazine

: 56138-36-4
3-methyl-4,6-diphenylpyridazine

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; caesium carbonate; In 1,4-dioxane; water; at 70 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jo401096u

Reference yield:

: 105537-53-9
4-phenyl-5-methyl-5-hydroxy-2(5H)-furanone

: 105538-79-2
6-Chloro-3-methyl-4-phenyl-pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / hydrazine hydrate / butan-1-ol / 12 h / Heating

2: phosphorus oxychloride / 4 h / 85 - 95 °C

With hydrazine hydrate; trichlorophosphate; In butan-1-ol;
DOI:10.1021/jm00385a003

Reference yield:

: 103-79-7,136675-26-8
1-phenyl-acetone

: 105538-79-2
6-Chloro-3-methyl-4-phenyl-pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: a) 135 deg C, 17 h, b) 117 deg C, 10 h

2: 89 percent / hydrazine hydrate / butan-1-ol / 12 h / Heating

3: phosphorus oxychloride / 4 h / 85 - 95 °C

With hydrazine hydrate; trichlorophosphate; In butan-1-ol;
DOI:10.1021/jm00385a003