C₁₇H₂₄BrISi

Base Information

Chemical Name:C₁₇H₂₄BrISi
CAS No.:864920-08-1
Molecular Formula:C₁₇H₂₄BrISi
Molecular Weight:463.272
Hs Code.:

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Chemical Property of C₁₇H₂₄BrISi

Chemical Property:

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Technology Process of C₁₇H₂₄BrISi

There total 4 articles about C₁₇H₂₄BrISi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: C₄H₁₀N^(1-)*C₁₇H₂₄BrN₂Si⁽¹⁺⁾

: 864920-08-1
C₁₇H₂₄BrISi

Guidance literature:: With iodine; methyl iodide; at 100 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2cc30417a

Reference yield:

: 29632-73-3
2-Bromo-4-iodoaniline

: 864920-08-1
C₁₇H₂₄BrISi

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 °C

1.2: 1 h / 0 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 3 h / Inert atmosphere

3.1: iodine; methyl iodide / 12 h / 100 °C / Inert atmosphere

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; triethylamine; sodium nitrite; methyl iodide; In water;
DOI:10.1039/c2cc30417a

Reference yield:

: 615-36-1
2-bromoaniline

: 864920-08-1
C₁₇H₂₄BrISi

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate / methanol; dichloromethane / 22 h

2.1: hydrogenchloride; sodium nitrite / water / 0 °C

2.2: 1 h / 0 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 3 h / Inert atmosphere

4.1: iodine; methyl iodide / 12 h / 100 °C / Inert atmosphere

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; N,N,N-trimethylbenzenemethanaminium dichloroiodate; triethylamine; calcium carbonate; sodium nitrite; methyl iodide; In methanol; dichloromethane; water;
DOI:10.1039/c2cc30417a