Technology Process of C24H31NO2
There total 3 articles about C24H31NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid; sodium cyanoborohydride / methanol / 16 h / 20 °C / Inert atmosphere
2: tetrahydrofuran / 48 h / Cooling with ice; Inert atmosphere
With
sulfuric acid; sodium cyanoborohydride;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201100535
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / 5 h / Reflux; Inert atmosphere
2: sodium acetate; oxalic acid / water / 10 h / 20 °C / Inert atmosphere
3: sulfuric acid; sodium cyanoborohydride / methanol / 16 h / 20 °C / Inert atmosphere
4: tetrahydrofuran / 48 h / Cooling with ice; Inert atmosphere
With
sulfuric acid; sodium acetate; oxalic acid; sodium cyanoborohydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; water;
DOI:10.1002/chem.201100535
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium acetate; oxalic acid / water / 10 h / 20 °C / Inert atmosphere
2: sulfuric acid; sodium cyanoborohydride / methanol / 16 h / 20 °C / Inert atmosphere
3: tetrahydrofuran / 48 h / Cooling with ice; Inert atmosphere
With
sulfuric acid; sodium acetate; oxalic acid; sodium cyanoborohydride;
In
tetrahydrofuran; methanol; water;
DOI:10.1002/chem.201100535
