gadolinium(III) acetate tetrahydrate

Base Information

Chemical Name:gadolinium(III) acetate tetrahydrate
CAS No.:14432-01-0
Molecular Formula:3C₂H₃O₂*Gd*4H₂O
Molecular Weight:406.445
Hs Code.:

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Chemical Property of gadolinium(III) acetate tetrahydrate

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Technology Process of gadolinium(III) acetate tetrahydrate

There total 2 articles about gadolinium(III) acetate tetrahydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: gadolinium(III) oxide

: 14432-01-0,15280-53-2,79464-08-7,100587-93-7,138481-01-3
gadolinium(III) acetate tetrahydrate

Guidance literature:: With water; acetic acid; In acetic acid; Gd2O3 was dissolved in glacial acetic acid; pH was controlled at 1; slowly evaporated at room temp.; after 3 days crystals were obtained; washed; elem. anal.; photoacoustic spectroscopy; IR;

Reference yield:

: gadolinium(III) nitrate nonahydrate

: 64-19-7,77671-22-8
acetic acid

: 14432-01-0,15280-53-2,79464-08-7,100587-93-7,138481-01-3
gadolinium(III) acetate tetrahydrate

Guidance literature:: In acetic acid; boiling nitrate in 50% HAc; recrystn. (H2O); elem. anal.;
DOI:10.1016/S0020-1693(98)00184-4

Reference yield: 90.0%

: HOOCCH₂N(CH₂CH₂N(CH₂COOH)CH₂CONHCH₂C₆H₁₀COOCH₂CH₂OCH₃)2

: 14432-01-0,15280-53-2,79464-08-7,100587-93-7,138481-01-3
gadolinium(III) acetate tetrahydrate

: (Gd(OOCCH₂N(CH₂CH₂N(CH₂COO)CH₂CONHCH₂C₆H₁₀COOCH₂CH₂OCH₃)2)(H₂O))*8H₂O

Guidance literature:: In pyridine; to soln. ligand in pyridine Gd(OAc)3*4H2O was added and stirred at 70°C for 6 h, solvent was stripped off, residue was taken in EtOH and refluxed for 2 h; react. mixt. was cooled and passed through Celite, solvent was removed, residue was taken in EtOH and added dropwise into acetone at 0°C,ppt. was filtered, washed with acetone, and dried in vacuo at 80.degree .C for 8 h; elem. anal.;
DOI:10.1039/b719440d