cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]

Base Information

Chemical Name:cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]
CAS No.:1333499-73-2
Molecular Formula:C₂₂H₁₇IN₂PdS
Molecular Weight:574.781
Hs Code.:

cis-[PdI(2,2'-bipyridine)(C<sub>6</sub>H<sub>4</sub>SPh-2)]

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Chemical Property of cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]

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Technology Process of cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]

There total 1 articles about cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 366-18-7
[2,2]bipyridinyl

: Pd2(dba)4

: 2236-42-2
(2-iodophenyl)(phenyl)thioether

: 1333499-73-2
cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]

Guidance literature:: In toluene; stirring of Pd2(dba)3*dba, 2,2'-bipyridine (2 equiv.) and IC6H4(SC6H4NO2-4)-2 (2.2 equiv.) in toluene under N2 for 18 h; evapn. of solvent, extn. with CH2Cl2, filtration, concn. to dryness, washing with Et2O, filtration; elem. anal.;
DOI:10.1021/om200607h

Reference yield: 97.0%

: 1333499-73-2
cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]

: 501-65-5
diphenyl acetylene

: 73491-36-8
thallium(I) triflate

: 1333500-04-1
[Pd(κ2-C,S-C(Ph)C(Ph)C6H4SPh-2)(2,2'-bipyridine)]TfO

Guidance literature:: In acetone; addn. of TlTfO to soln. of PdI(bipy)(C6H4SPh) and PhCCPh in acetone, stirring for 1 h; filtration, concn., addn. of Et2O, filtration, washing with Et2O; elem. anal.;
DOI:10.1021/om200607h

Reference yield: 96.0%

: 503-17-3
dimethylacetylene

: 1333499-73-2
cis-[PdI(2,2'-bipyridine)(C₆H₄SPh-2)]

: 73491-36-8
thallium(I) triflate

: 1333500-06-3
[Pd(κ2-C,S-C(Me)C(Me)C6H4SPh-2)(2,2'-bipyridine)]TfO

Guidance literature:: In acetone; addn. of TlTfO to soln. of PdI(bipy)(C6H4SPh) and MeCCMe in acetone, stirring for 1 h; filtration, concn., addn. of Et2O, filtration, washing with Et2O; elem. anal.;
DOI:10.1021/om200607h