1,3-dibenzyl perhydrobenzimidazolinium chloride

Base Information

Chemical Name:1,3-dibenzyl perhydrobenzimidazolinium chloride
CAS No.:1446520-81-5
Molecular Formula:C₂₁H₂₅N₂*Cl
Molecular Weight:340.896
Hs Code.:

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Chemical Property of 1,3-dibenzyl perhydrobenzimidazolinium chloride

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Technology Process of 1,3-dibenzyl perhydrobenzimidazolinium chloride

There total 3 articles about 1,3-dibenzyl perhydrobenzimidazolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 135613-88-6,143443-23-6,65838-10-0,191480-61-2
cis/trans-N,N'-dibenzylcyclohexane-1,2-diamine

: 122-51-0
orthoformic acid triethyl ester

: 1446520-81-5
1,3-dibenzyl perhydrobenzimidazolinium chloride

Guidance literature:: With ammonium chloride; at 110 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.3987/COM-13-12678

Reference yield:

: 100-52-7
benzaldehyde

: 1446520-81-5
1,3-dibenzyl perhydrobenzimidazolinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3 h / Reflux

2: sodium tetrahydroborate / methanol / 13.5 h / 20 °C / Reflux

3: ammonium chloride / 12 h / 110 °C / Inert atmosphere; Schlenk technique

With sodium tetrahydroborate; ammonium chloride; In methanol; ethanol;
DOI:10.3987/COM-13-12678

Reference yield:

: 694-83-7
rac-diaminocyclohexane

: 1446520-81-5
1,3-dibenzyl perhydrobenzimidazolinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3 h / Reflux

2: sodium tetrahydroborate / methanol / 13.5 h / 20 °C / Reflux

3: ammonium chloride / 12 h / 110 °C / Inert atmosphere; Schlenk technique

With sodium tetrahydroborate; ammonium chloride; In methanol; ethanol;
DOI:10.3987/COM-13-12678