(2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride

Base Information

Chemical Name:(2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride
CAS No.:1014625-63-8
Molecular Formula:C₂₅H₃₁ClNPPd
Molecular Weight:518.375
Hs Code.:

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Chemical Property of (2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride

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Technology Process of (2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride

There total 1 articles about (2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.7%

: bis(η3-allyl-μ-chloropalladium(II))

: 1014625-59-2
2-diphenylphosphinocyclopentene-1-(tert-butyl)imine

: 1014625-63-8
(2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride

Guidance literature:: In dichloromethane; std. Schlenk technique; soln. of ligand in CH2Cl2 was added to soln. of Pd complex in CH2Cl2; stirred at room temp. for 14 h; volatiles removed (vac.); triturated with pentane; dissolved in Et2O; cooled to -25°C; elem. anal.;
DOI:10.1021/om701106q

Reference yield: 89.7%

: 1014625-63-8
(2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 1014625-65-0
(2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) triflate

Guidance literature:: In dichloromethane; byproducts: AgCl; std. Schlenk technique; soln. of Pd complex in CH2Cl2 was added to suspn. of Ag salt in CH2Cl2; stirred for 2 h in dark; volatiles removed (vac.); triturated with pentane; extd. (THF); filtered; solvent removed (vac.); triturated with pentane; elem. anal.;
DOI:10.1021/om701106q

Reference yield: 87.2%

: ammonium hexafluorophosphate

: 1014625-63-8
(2-diphenylphosphinocyclopentene-1-(tert-butyl)imine)(allyl)palladium(II) chloride

: 1147880-83-8
[((C₆H₅)2PC₅H₆CHNC(CH₃)3)Pd(CH₂CHCH₂)]⁽¹⁺⁾*PF₆^(1-)=[((C₆H₅)2PC₅H₆CHNC(CH₃)3)Pd(CH₂CHCH₂)]PF₆

Guidance literature:: In dichloromethane; std. Schlenk technique; soln. of Pd complex in CH2Cl2 was added to stirred slurry of B compd. in CH2Cl2; mixt. was stirred for 14 h at ambient temp.; evapd. (vac.); washed (Et2O); elem. anal.;
DOI:10.1021/om900066t