C₂₅H₃₀F₂N₄O₉

Base Information

Chemical Name:C₂₅H₃₀F₂N₄O₉
CAS No.:1422423-86-6
Molecular Formula:C₂₅H₃₀F₂N₄O₉
Molecular Weight:568.531
Hs Code.:

C<sub>25</sub>H<sub>30</sub>F<sub>2</sub>N<sub>4</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₂₅H₃₀F₂N₄O₉

Chemical Property:

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Technology Process of C₂₅H₃₀F₂N₄O₉

There total 8 articles about C₂₅H₃₀F₂N₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3054-95-3
acrylaldehyde diethyl acetal

: C₂₂H₂₈F₂N₄O₉

: 1422423-81-1
C₂₅H₃₀F₂N₄O₉

: 1422423-86-6
C₂₅H₃₀F₂N₄O₉

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 40 ℃; for 4h; Overall yield = 1680 mg; Inert atmosphere;
DOI:10.1002/chem.201200859

Reference yield:

: 22037-27-0
3-allyl-5-nitrosalicylaldehyde

: 1422423-81-1
C₂₅H₃₀F₂N₄O₉

: 1422423-86-6
C₂₅H₃₀F₂N₄O₉

Guidance literature:: Multi-step reaction with 6 steps

1: sodium methylate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 20 °C / Inert atmosphere

3: zinc; acetic acid / 0.25 h / 20 °C

4: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 0.75 h / 5 °C

5: sodium methylate / methanol / 8 h / 20 °C / Inert atmosphere

6: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 4 h / 40 °C / Inert atmosphere

With tert.-butylnitrite; diethylamino-sulfur trifluoride; trimethylsilylazide; camphor-10-sulfonic acid; sodium methylate; acetic acid; zinc; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201200859

Reference yield:

: 97-51-8
5-Nitrosalicylaldehyde

: 1422423-81-1
C₂₅H₃₀F₂N₄O₉

: 1422423-86-6
C₂₅H₃₀F₂N₄O₉

Guidance literature:: Multi-step reaction with 8 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate / acetonitrile / 6 h / Reflux

2: 4 h / 200 °C

3: sodium methylate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

4: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 20 °C / Inert atmosphere

5: zinc; acetic acid / 0.25 h / 20 °C

6: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 0.75 h / 5 °C

7: sodium methylate / methanol / 8 h / 20 °C / Inert atmosphere

8: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 4 h / 40 °C / Inert atmosphere

With tert.-butylnitrite; diethylamino-sulfur trifluoride; trimethylsilylazide; camphor-10-sulfonic acid; sodium methylate; tetra-(n-butyl)ammonium iodide; potassium carbonate; acetic acid; zinc; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: |Claisen Rearrangement;
DOI:10.1002/chem.201200859