[Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO₄

Base Information

Chemical Name:[Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO₄
CAS No.:604757-00-8
Molecular Formula:C₄₂H₃₀CdN₄O₅P*ClO₄
Molecular Weight:913.558
Hs Code.:

[Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO<sub>4</sub>

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Chemical Property of [Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO₄

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Technology Process of [Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO₄

There total 1 articles about [Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 50890-67-0
4,5-Diazafluoren-9-one

: cadmium(II) acetate tetrahydrate

: sodium perchlorate

: 64-19-7,77671-22-8
acetic acid

: 603-35-0
triphenylphosphine

: 604757-00-8
[Cd(4,5-diazafluoren-9-one)2(triphenylphosphine oxide)(acetate)]ClO₄

Guidance literature:: With air; In ethanol; addn. of acetic acid to a soln. of Cd salt and 4,5-diazafluoren-9-one inabsolute ethanol, refluxing on a water bath for 3 h, addn. of triphenyl phosphine in benzene, refluxing for 1 h, addn. of NaClO4 in ethanol, refluxing for 10 min; leaving overnight, filtration, natural evapn. of the filtrate at room temp. over half year, filtration, washing with ether, natural drying; elem. anal.;
DOI:10.1016/S0022-2860(03)00325-9