C₃₀H₂₉ClO₈

Base Information

Chemical Name:C₃₀H₂₉ClO₈
CAS No.:1616873-07-4
Molecular Formula:C₃₀H₂₉ClO₈
Molecular Weight:553.008
Hs Code.:

C<sub>30</sub>H<sub>29</sub>ClO<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₂₉ClO₈

Chemical Property:

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Technology Process of C₃₀H₂₉ClO₈

There total 12 articles about C₃₀H₂₉ClO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616873-09-6
C₂₃H₂₅ClO₇

: 98-88-4
benzoyl chloride

: 1616873-07-4
C₃₀H₂₉ClO₈

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201402254

Reference yield:

: C₂₅H₃₃ClO₉

: 1616873-07-4
C₃₀H₂₉ClO₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 20 h / 65 °C / Inert atmosphere

2.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

4.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

4.2: 0.33 h

5.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

With hydrogenchloride; dmap; water; sodium acetate; toluene-4-sulfonic acid; acetic acid; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1002/chem.201402254

Reference yield:

: 1616873-73-4
C₂₀H₂₁ClO₇

: 1616873-07-4
C₃₀H₂₉ClO₈

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

1.2: 0.33 h

2.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

With dmap; toluene-4-sulfonic acid; triethylamine; In dichloromethane; acetone;
DOI:10.1002/chem.201402254