C₂₉H₄₂N₆O₁₁S₂

Base Information

• Chemical Name: C₂₉H₄₂N₆O₁₁S₂
• CAS No.: 1611498-13-5
• Molecular Formula: C₂₉H₄₂N₆O₁₁S₂
• Molecular Weight: 714.818
• Mol file: 1611498-13-5.mol

Synonyms:

Chemical Property of C₂₉H₄₂N₆O₁₁S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₄₂N₆O₁₁S₂

There total 11 articles about C₂₉H₄₂N₆O₁₁S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fmoc-Val-OH (68858-20-8) → C29H42N6O11S2 (1611498-13-5)

Guidance literature:

Multi-step reaction with 5 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl acetamide

2: sodium hydrogencarbonate / water; tetrahydrofuran

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl acetamide

4: diethylamine / 1-methyl-pyrrolidin-2-one

5: 1-methyl-pyrrolidin-2-one

With sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; N,N-dimethyl acetamide; water;

Reference yield:

C16H21NO9S2 → C29H42N6O11S2 (1611498-13-5)

Guidance literature:

Multi-step reaction with 3 steps

1: methanesulfonic acid / toluene; 1,2-dichloro-ethane / 120 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl acetamide

3: 1-methyl-pyrrolidin-2-one

With methanesulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1-methyl-pyrrolidin-2-one; N,N-dimethyl acetamide; 1,2-dichloro-ethane; toluene;

Reference yield:

methyl 6-mercapto-4-thiahexanoate (201991-10-8) → C29H42N6O11S2 (1611498-13-5)

Guidance literature:

Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / 45 °C

2: potassium permanganate; dihydrogen peroxide; 18-crown-6 ether / dichloromethane

3: sodium carbonate / N,N-dimethyl acetamide

4: methanesulfonic acid / toluene; 1,2-dichloro-ethane / 120 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl acetamide

6: 1-methyl-pyrrolidin-2-one

With potassium permanganate; methanesulfonic acid; 18-crown-6 ether; dihydrogen peroxide; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl acetamide; 1,2-dichloro-ethane; toluene;

upstream raw materials:

C₁₁H₁₅NO₈S₂

(2S)-2-[[(2S)-2-amino-3-methylbutanoyl]amino]-N-[4-(hydroxymethyl)phenyl]-5-ureidopentanamide

C₁₅H₁₈N₂O₁₀S₂

Fmoc-Val-OH

Downstream raw materials:

C₃₆H₄₅N₇O₁₅S₂