((C₆H₅)2GeH)2(CH₂)3

Base Information

Chemical Name:((C₆H₅)2GeH)2(CH₂)3
CAS No.:151920-29-5
Molecular Formula:C₂₇H₂₈Ge₂
Molecular Weight:497.699
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2GeH)2(CH<sub>2</sub>)3

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Chemical Property of ((C₆H₅)2GeH)2(CH₂)3

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Technology Process of ((C₆H₅)2GeH)2(CH₂)3

There total 1 articles about ((C₆H₅)2GeH)2(CH₂)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120154-42-9
diphenylhydrogermyllithium

: 109-64-8
1,3-dibromo-propane

: 151920-29-5
((C₆H₅)2GeH)2(CH₂)3

Guidance literature:: With water; In tetrahydrofuran; byproducts: (C6H5)2GeH2, (C6H5)2HGeBr; under N2 or Ar, slow addn. ofr the org. compd. in THF to a soln. of the germyllithium in THF at -40°C, 10 min at this temp., heating to ambient temp., 3 h stirring at 20°C, hydrolysis, further byproduct: LiBr; extn., drying over anhydrous Na2SO4, concg. in vac., not isolated, 1H NMR;
DOI:10.1016/S0020-1693(00)92307-7

Reference yield: 26.0%

: 151920-29-5
((C₆H₅)2GeH)2(CH₂)3

: 151920-28-4
((C₆H₅)2GeCH₂)2CH₂

Guidance literature:: With dibutylmercury; In benzene; byproducts: BuH, Hg; under N2 or Ar, stirring a benzene soln. of the germyl compd. and dibutylmercury for 4 h at 40°C in the dark, heating the formed mercuric compd. in a Carius tube for 12 h at 120°C; elimination of Hg, concg., recrystn. (1:5 ether/pentane), decantation, drying under vac.;
DOI:10.1016/S0020-1693(00)92307-7