[RuCp(AsPh₃)(CH₃CN)2]PF₆

Base Information

Chemical Name:[RuCp(AsPh₃)(CH₃CN)2]PF₆
CAS No.:365979-54-0
Molecular Formula:C₂₇H₂₆AsN₂Ru*F₆P
Molecular Weight:699.473
Hs Code.:

[RuCp(AsPh<sub>3</sub>)(CH<sub>3</sub>CN)2]PF<sub>6</sub>

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Chemical Property of [RuCp(AsPh₃)(CH₃CN)2]PF₆

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Technology Process of [RuCp(AsPh₃)(CH₃CN)2]PF₆

There total 1 articles about [RuCp(AsPh₃)(CH₃CN)2]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate

: 603-32-7
triphenyl-arsane

: 365979-54-0
[RuCp(AsPh₃)(CH₃CN)2]PF₆

Guidance literature:: In dichloromethane; (Ar); stirring a soln. of ruthenium complex and arsine in CH2Cl2 at roomtemp. for 2 h; concn., addn. of Et2O, filtration, washing with Et2O, drying in vac.; elem. anal.;
DOI:10.1016/S0022-328X(01)01487-5

Reference yield: 97.0%

: 365979-54-0
[RuCp(AsPh₃)(CH₃CN)2]PF₆

: 106-95-6
allyl bromide

: 455884-01-2
[C₅H₅RuBr(As(C₆H₅)3)CH₂CHCH₂]⁽¹⁺⁾*PF₆^(1-)=[C₅H₅RuBr(As(C₆H₅)3)CH₂CHCH₂]PF₆

Guidance literature:: In dichloromethane; (Ar); addn. of allyl bromide to a soln. of ruthenium complex in CH2Cl2, stirring at room temp. for 5 h; evapn., dissolving in CH2Cl2, addn. of hexane, filtration, washing with hexane, drying in vac.; elem. anal.;
DOI:10.1016/S0022-328X(01)01487-5

Reference yield: 33.0%

: 365979-54-0
[RuCp(AsPh₃)(CH₃CN)2]PF₆

: [(η(5)-C5H5)Ru(η(6)-benzene)](1+)

: 455884-10-3
[C₅H₅Ru(As(C₆H₅)3)2(CH₃CN)]⁽¹⁺⁾*PF₆^(1-)=[C₅H₅Ru(As(C₆H₅)3)2(CH₃CN)]PF₆

Guidance literature:: In benzene; (Ar); stirring a soln. of ruthenium complex in C6H6 at 80°C for 30 min; evapn., column chromy. (SiO2, CH2Cl2/acetone 10:1 vol.), evapn., drying in vac.;
DOI:10.1016/S0022-328X(01)01487-5