Technology Process of 1-isopropyl-3-cyclohexyl-3,4-dihydroquinazolinium-2-dithiocarboxylate
There total 6 articles about 1-isopropyl-3-cyclohexyl-3,4-dihydroquinazolinium-2-dithiocarboxylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hexamethylsilazane;
In
tetrahydrofuran; hexane;
at -40 - 20 ℃;
for 2h;
Schlenk technique;
DOI:10.1021/om300887y
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ethanol / Reflux; Schlenk technique
2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux; Schlenk technique
3: ammonium chloride / 120 °C / Schlenk technique
4: acetone / 8 h / Schlenk technique
5: potassium hexamethylsilazane / hexane; tetrahydrofuran / 2 h / -40 - 20 °C / Schlenk technique
With
lithium aluminium tetrahydride; potassium hexamethylsilazane; ammonium chloride;
In
tetrahydrofuran; ethanol; hexane; acetone;
DOI:10.1021/om300887y
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux; Schlenk technique
2: ammonium chloride / 120 °C / Schlenk technique
3: acetone / 8 h / Schlenk technique
4: potassium hexamethylsilazane / hexane; tetrahydrofuran / 2 h / -40 - 20 °C / Schlenk technique
With
lithium aluminium tetrahydride; potassium hexamethylsilazane; ammonium chloride;
In
tetrahydrofuran; hexane; acetone;
DOI:10.1021/om300887y
