C₃₃H₄₂O₉

Base Information

Chemical Name:C₃₃H₄₂O₉
CAS No.:1392098-20-2
Molecular Formula:C₃₃H₄₂O₉
Molecular Weight:582.691
Hs Code.:

C<sub>33</sub>H<sub>42</sub>O<sub>9</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₂O₉

Chemical Property:

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Technology Process of C₃₃H₄₂O₉

There total 20 articles about C₃₃H₄₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 1392098-17-7
C₃₉H₅₄O₁₂

: 1392098-20-2
C₃₃H₄₂O₉

Guidance literature:: With Dowex; In methanol; at 50 ℃; for 20h;
DOI:10.3762/bjoc.8.82

Reference yield:

: 934243-80-8
2-iodo-3,5-bis(phenylmethoxy)benzenemethanol

: 1392098-20-2
C₃₃H₄₂O₉

Guidance literature:: Multi-step reaction with 12 steps

1.1: pyridine / dichloromethane / 3 h / 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium t-butanolate / toluene / Inert atmosphere

2.2: 6 h / 50 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 1.08 h / -78 - 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate / tetrahydrofuran / 1.5 h / 20 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 96 h / 20 °C

7.1: tri-n-butylamine hydrofluoride / tetrahydrofuran / 48 h / 20 °C

8.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 72 h / 20 °C

9.1: N,N-dimethyl-formamide / 1.5 h / -40 °C

9.2: 0.5 h / -40 - 20 °C

10.1: dmap / toluene / 3 h / 20 °C

11.1: tri-n-butylamine hydrofluoride / tetrahydrofuran / 48 h / 20 °C

12.1: Dowex / methanol / 20 h / 50 °C

With pyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; palladium 10% on activated carbon; hydrogen; tri-n-butylamine hydrofluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; tetra-n-butylammoniumfluoride trihydrate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.3762/bjoc.8.82

Reference yield:

: 934243-67-1
2-iodo-3,5-bis(phenylmethoxy)-(2',2'-dimethylpropanoyloxymethyl)benzene

: 1392098-20-2
C₃₃H₄₂O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium t-butanolate / toluene / Inert atmosphere

1.2: 6 h / 50 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 1.08 h / -78 - 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate / tetrahydrofuran / 1.5 h / 20 °C

5.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 96 h / 20 °C

6.1: tri-n-butylamine hydrofluoride / tetrahydrofuran / 48 h / 20 °C

7.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 72 h / 20 °C

8.1: N,N-dimethyl-formamide / 1.5 h / -40 °C

8.2: 0.5 h / -40 - 20 °C

9.1: dmap / toluene / 3 h / 20 °C

10.1: tri-n-butylamine hydrofluoride / tetrahydrofuran / 48 h / 20 °C

11.1: Dowex / methanol / 20 h / 50 °C

With dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; palladium 10% on activated carbon; hydrogen; tri-n-butylamine hydrofluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; tetra-n-butylammoniumfluoride trihydrate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.3762/bjoc.8.82