tri-sec-butyl orthoformate

Base Information

• Chemical Name: tri-sec-butyl orthoformate
• CAS No.: 17159-00-1
• Molecular Formula: C₁₃H₂₈O₃
• Molecular Weight: 232.364
• Mol file: 17159-00-1.mol

Synonyms:

Chemical Property of tri-sec-butyl orthoformate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tri-sec-butyl orthoformate

There total 2 articles about tri-sec-butyl orthoformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

orthoformic acid triethyl ester (122-51-0) → orthoformic acid tri-((S)-sec-butyl ester) (16754-48-6,17159-00-1)

Guidance literature:

unter Entfernen des entstehenden Aethanols;

DOI:10.1021/ja01132a502

Reference yield:

orthoformic acid triethyl ester (122-51-0) + iso-butanol (78-92-2,15892-23-6) → optically inactive orthoformic acid tri-sec-butyl ester (16754-48-6,17159-00-1)

Guidance literature:

DOI:10.1021/ja01122a502

Reference yield: 96.0%

3-phenyl-propionaldehyde (104-53-0) + tri-sec-butyl orthoformate (16754-48-6,17159-00-1) → C17H28O2 (1146221-11-5)

Guidance literature:

With cerium triflate; In isopropyl alcohol; toluene; at 20 ℃; for 0.166667h;

DOI:10.1055/s-0028-1087534

upstream raw materials:

orthoformic acid triethyl ester

iso-butanol

Downstream raw materials:

1-chloro-4-(di-sec-butoxy-methoxy)-benzene

N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester

sec-butyl formate

Di(s-butyl) carbonate